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Despite the high overall yield in the described solid phase approach, it has several drawbacks for the scale-up process such as the application of the highly toxic and corrosive hydrogen fluoride for cleavage of the peptide from the resin, low loading (0.300.35 mmol/g of resin) proved necessary for successful on-resin cyclization, and the use of excess amounts of reagents (3-fold of DIC, 2.4-fold of HOBt, etc.) on each step

Of particular interest are protein supplements, the global market for which is rapidly expanding and estimated to reach US $21.5 billion by 2025 (73)

However, this reward system can sometimes lead to unhealthy behaviors

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